EDX 3600B Energy Dispersive X-ray Fluorescence Spectrometer

X-ray fluorescence (XRF) is a powerful analytical technique used in a wide variety of industries to determine the elemental composition of various materials. XRF analyzers are widely recognised as a means for accurate, rapid, and non-destructive testing.

The Skyray EDX3600B is a high-end energy dispersive XRF spectrometer (EDXRF) with a large sample chamber which supports most sample sizes. The system comes with a vacuum pump for light element detection and a helium injection system for liquids analysis. The Skyray EDX3600B is a multifunctional rapid analyzer applicable to a variety of applications (some are listed below).

The system comes with easy-to-operate software suitable for all users. The software highlights all the information a user may require on one screen including elemental spectrum, measurement time, sample image and real-time test results, critical instrument data and more. Furthermore, this system provides a colour camera system for simple sample alignment and viewing. In only 10 seconds the operator can see the main elements contained in a sample. Full results are available after a short additional period.

Mineral (ore) analysis
  1. Minerals (Mg, Al, K, Ca, Ti, V, Cr, Mn, Fe, Co, Ni, Cu, Zn, Se, Zr, Nb, Mo, Pd, Ag, Cd, Sn, Sb, In, Ba, Hf, Ta, Pt, Au, Pb, Bi, etc.)
  2. Slags, Feeds, Concentrates, and Tailings
  3. Phosphate rock and fertilizer (P, S, Ca, Fe)
  4. Kaolin and other Clays (Mg, Al, Si, Ca, Ti, Fe)
  5. Gypsum (Ca, S), Dolomite(Ca, Mg), Limestone (Ca)
Metal identification
  1. Alloy Analysis:
    1. Iron alloys (e.g. stainless, high-temperature, tool steels)
    2. nonferrous metal (Al, Ti, Cr, Ni, Cu, Zn, Cd, Zr, Sn, Mo, Pb, etc.)
  2. Precious Metal Materials (Au, Ag, Pt, Pd, Ru, Rh, W, Os, Ir, etc.)
  3. Silicon metal
  4. Metal foil thickness
RoHS compliance screening

Detection of concentrations for Pb, Cd, Hg, total Cr and total Br for most products directly affected by RoHS directive including:

Consumer equipment, household appliances, IT and telecommunications equipment, lighting equipment, electrical and electronic tools, toys, leisure and sports equipment, medical devices, monitoring and control instruments, automatic dispensers, etc.

Pharmaceutical Applications (solution, pellet, chip, powder)
  1. Iodine, selenium, copper, cobalt in sterilization products
  2. Hazardous metal analysis in pharmaceuticals

Specifications:

Analyzable element range

11Na (sodium) ~ 92U (uranium)

Analyzable element content

Dynamic from ppm-level to nearly 100 percent

Simultaneous analytical ability

Maximum 24 elements at a time

Acceptable sample form

Solid, powder, pellet, liquid

Test time

60sec ~ 200sec (extra 50sec if vacuum required)

Sample chamber

Atmosphere

Air, vacuum or helium

Inside dimension

320mm (diam) x 180mm (height)

Environmental requirements

Temperature

15°C ~ 30°C

Relative humidity

35% ~ 70% (no condensation) 

Others

Free of particles, corrosive gases, perceptible vibration

Power requirements

AC 220V/110V ±5V, 50Hz (optional AC purified regulatory power supply)

Dimensions of spectrometer

650(W) x 466(H) x 608(D) mm

Net weight

Spectrometer

Approx. 105 kg

Vacuum pump

Approx. 25 kg

Main Features:

  1. Large-volume sample chamber able to accept most different sized samples.

  2. Inbuilt high-resolution camera sample viewing system provides easy sample alignment.

  3. Newest version of application software provides all the critical information on one screen. Display element spectrum, in-process results of elemental content, camera image, measurement time, etc

  4. Vacuuming system for sample chamber enhances detection sensitivity of light elements (Na, Mg, Al, Si, etc).

  5. High stability SpellmanTM high voltage supply with maximum 50KV voltage. Ensure lifetime working stability; adjustable voltage can excite specific elements of interest in best status.

  6. High excitation efficiency Oxford™ 50W X-ray tube. Provides high-efficiency X-ray source, high power performs low detection limits for certain covered elements.

  7. High cost-performance thermoelectric cooling Si-PIN detector as standard configurations for general test requirements, and optional advanced Silicon Drift Detector (SDD) of excellent energy resolution for better test accuracy and precision.

  8. Inbuilt signal-to-noise enhancer realizes 25 times improvement of effective signal processing.

Main Configurations:

High voltage supply

Manufacturer

Spellman High Voltage Electronics Corporation (USA)

Maximum Voltage

50kV

Stability

0.001% per 8 hours (temperature: 20°C ±0.2°C)

X-ray tube

Manufacturer

Oxford Instruments Plc (USA)

Tube voltage

4kV – 50kV

Tube current

50μA – 1000μA

Stability

0.2% over 4 hours

Primary filters

Automatic selection from among 5 types of filters.

Collimators

Switching style

Automatic

Pore diameter range

⌀0.2, ⌀0.5, ⌀1.0, ⌀2.0, ⌀3.0, ⌀4.0, ⌀6.0, ⌀8.0 (mm)

Detection system (alternative)

Type

Thermoelectric cooling Silicon PIN detector (Si-PIN)

Thermoelectric cooling silicon drift detector (SDD)

Energy Resolution

Si-PIN detector: 150±5eV (Mn K-alpha)

SDD detector: 140±5eV (Mn K-alpha)

Signal-to-noise enhancer

Realize 25 times enhancement of effective signal processing

Multi-channel analyzer

A time-resolved multi-channel analyzer produces accumulating digital spectrum.

High resolution camera

Inbuilt 3 million pixels CCD camera for sample observation

Evacuation system

Oil vacuum pump

3 liters Dewar capacity

Pressure monitor

With pressure sensor

Software

Qualitative analysis

Measurement and analysis of measured data

Quantitative analysis

Calibration curve method, matrix correction

Utility

Automatic correction for intensity and energy

Monitoring of operating condition of the instrument

Function of tabulating the results of analysis