EDX3000 Energy Dispersive X-ray Fluorescence Spectrometer

X-ray fluorescence (XRF) is a powerful analytical method used in a wide variety of industries to determine the elemental composition of various materials. One use of XRF that has gained substantial interest is its ability to accurately, nondestructively and rapidly detect precious metals content in many kinds of materials such jewelry, bullion, nugget, ingot and scrap as well as in liquids. An XRF test is much fast than fire assay work and more accurate than other options.

The EDX3000 is a benchtop XRF spectrometer providing a complete solution for full precious metals analysis for jewellers, precious metal refiners and recyclers, banks, etc. Some popular desktop instruments for precious metal analysis require Liquid Nitrogen (LN2) to cool their detection systems. However, LN2 is a hassle for the user as well as an added expense. Because of that, Skyray XRF has developed our gold tester and precious metal analyzers so that they do not require LN2 but still provide excellent performance.

The EDX3000 system incorporates a high energy resolution Si-PIN detector which allows it to properly separate peaks of all precious metals and provide accurate information on the content of each as required, so it’s able to detect both full precious metals (Au, Ag, Pt, Pd, Ru, Rh, W, Os, Ir, etc.) and base metals (Cr, Mn, Fe, Co, Ni, Cu, Zn, Cd, Sn, Pb, etc.) simultaneously.

Furthermore, the software package for EDX3000 has been developed specifically for full precious metal analysis; providing easy navigation and report generation as required by users that don’t have a technical background. It is everything that refiners, jewellers, and serious buy-back organizations engaged in full precious metal property need. The user-friendly software highlights all the information a user requires on one screen including measurement time, a screenshot of the sample, critical instrument data, in-process results, etc. The EDX3000 can identify gold karat rating in as little as 10 seconds and provide a complete elemental composition in 60–300 seconds.

For these reasons the EDX3000 is particularly suited to refiners or serious buy-back organisations. Those who are buying back jewellery primarily for the gold content will typically consider the more specialised EDX600 because of its low cost. The accuracy, pricing and software of EDX3000 set it apart from all other nondestructive precious metal analysers as well as from destructive chemical test methods.

Another application for EDX3000 is the plating and plating bath for monitoring plating thickness. The inclusion of a high energy resolution Si-PIN detector and matching thickness analysis software allows it to measure multiple metal coating layers of complicated elemental compositions. The following common elements are measurable, although virtually any plating and plating bath can be analyzed: Gold, Platinum, Rhodium, Iridium, Titanium, Chromium, Chromate, Nickel, Sn-Pb Solder.

Specifications:

Analyzable element range

19K (potassium) – 92U (uranium)

Analyzable element content

Dynamic from ppm-level to nearly 100 percent

Metal elements of interest

Precious metals

Au, Ag, Pt, Pd, Ru, Rh, W, Os, Ir, etc.

Base metals

Cr, Mn, Fe, Co, Ni, Cu, Zn, Cd, Sn, Pb, etc.

Acceptable sample type

Solid, powder, liquid (solution, suspension)

Dimension of sample chamber

260(W) x 90(H) x 310(D) mm

Test time

60sec ~ 300sec

Precision (repeatability)

RSD≤0.05% for element content ≥90%

RSD≤0.12% for element content ≥ 75%

RSD≤0.30% for element content ≥ 50%

Environmental requirements

Temperature

15°C ~ 30°C (air-conditioner recommended)

Relative humidity

35% ~ 70%

Others

Free of particles, corrosive gases, perceptible vibration

Power requirements

AC 220V±5V, 50/60HZ (optional AC purified regulatory power supply)

Outside dimensions

530(W) x 380(H) x 370(D) mm

Net weight

Approx. 32 kg

Main Features:

  1. Colour camera sample viewing system provides easy sample alignment.

  2. Latest application software provides all the critical information on one screen. Display spectrum, in-process results of precious metal content, camera image, measurement time, etc

  3. As a full precious metal analyzer, EDX3000 provides repeatability with a standard deviation around 0.05% (performance can vary based on instrument set-up, elements tested for, quality of reference standards, etc.).

  4. Test reports are exported by software into Excel file for easy data backup.

  5. High stability Spellman™ high voltage supply with maximum 50kV improves lifetime working stability; adjustable voltage can target specific elements of interest.

  6. World-leading thermoelectric cooling Si-PIN detector with high energy resolution. Provides excellent resolution among elements of close XRF energy with high repeatability.

Main Configurations:

High voltage supply

Manufacturer

Spellman High Voltage Electronics Corporation (USA)

Maximum Voltage

50KV

Stability

0.002% per 8 hours (temperature: 20°C ±0.2°C)

X-ray tube

Target material

Rhodium, Tungsten (optional)

Tube voltage

5KV ~ 50KV

Tube current

50μA ~ 1000μA

Collimators

Manual switch collimators of different apertures

Primary filters

Manual selection from among 5 types of filters

Detection system

Type

Thermoelectric cooling Si-PIN semiconductor detector

Energy Resolution

155±5eV (Mn K-alpha)

Amplifier circuit

One preset & one main amplifier circuits (in the detector)

Multi-channel analyzer

(MCA)

A time-resolved multi-channel analyzer produces accumulating digital spectrum.

Multi-channel analyzer

A time-resolved multi-channel analyzer produces accumulating digital spectrum.

Sample camera

3 million pixels CCD camera for sample observation with maximum 30 magnification times

Software

Qualitative analysis

Measurement and analysis of measured data

Quantitative analysis

Calibration curve method, matrix correction

Utility

Automatic correction for intensity and energy

Monitoring of operating condition of the instrument

Function of tabulating the results of analysis